1. Wear eye protection and gloves (leather or thick rubber).
2. The hole in the stopper should be only slightly
smaller than the tubing.
Be sure the ends of the tubing are fire-polished
(unpolished tubing is almost impossible to insert into a stopper without
requiring a dangerously high amount of force).
Lubricate the hole and the end of the glass
tubing. Good lubricants include glycerin, water, soap, stopcock grease, or
soapy water. Use only a little, and choose a lubricant which will not
react with any of the chemicals you plan on using with the apparatus.
Keep
hand on tubing close to the stopper and out of line with the end of the
tube. Do NOT use your palm.
DO NOT FORCE THE TUBING. If you cannot easily get
the tubing through the stopper, change lubricants or make the hole bigger.
Rotate the tubing as you insert it slowly. Add
extra lubricant as needed.
Do not rock the tubing back and forth. This can
easily shatter the tubing.
When stoppers and glass tubing become sealed
together, they must not be separated by force. Either cut the stopper
loose or discard the equipment.
CUTTING
A GLASS ROD OR TUBING
1.
Always
wear eye protection!
2.
Score
the glass only once, firmly. Multiple score lines will usually result in jagged
breaks, or cause the end to shatter while snapping it.
3.
Use
the correct tool for scoring. A hardened triangular file, or a special tungsten
carbide or diamond-edged scoring blade will work. Glass is very hard, and will
only snap cleanly with a sharp score line.
4.
Never
hold the glass with bare hands while snapping it. Use heavy gloves if
available, and wrap the glass in a cloth. The cloth will serve to catch the
slivers which invariably are produced during snapping.
5.
Anything
with a diameter greater than 10 mm should be cut with a glass saw.
6.
Fire
polish the ends.
MISCELLANEOUS
Glass gets EXTREMELY HOT, and you can't tell how
hot it is by looking at it. So use
hot pads, insulated hot mitts or gloves.
Leave a warning note for others in the area.
Don't lay hot glass on cold surfaces or in water.
It will crack easily, wasting your work and possibly hurting someone.
Keep glass moving and rotating in a flame. Don't
let the flame sit on one spot for more than a moment. Glass can shatter if
it is heated unevenly.
Eye protection should be worn when working with
glassware.
DISPOSAL
Inspect before use and discard broken, chipped or
cracked glassware.
Never handle broken glass with your bare
hands. Use a brush and dustpan to
clean up broken glass immediately. Forceps or tape can be used to pick up
smaller pieces.
Dispose of all uncontaminated glassware (non-hazardous,
non-pathological, non-radioactive) in the appropriate manner (NOT in the
black garbage bags).